Enviar artigo por via de e-mail STRUCTURAL FEATURES OF TRIS(ETHYLENEDIAMINE)NICKEL(II) DICHLOROIDE DIHYDRATE SINGLE CRYSTALS IN THE TEMPERATURE RANGE 85–293 K
- Autores: Sorokina N.I.1, Komornikov V.A.1, Verin I.A.1, Novikova N.E.1
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Afiliações:
- Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”
- Edição: Volume 70, Nº 5 (2025)
- Páginas: 732-735
- Seção: СТРУКТУРА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
- URL: https://cardiosomatics.ru/0023-4761/article/view/693866
- DOI: https://doi.org/10.31857/S0023476125050032
- EDN: https://elibrary.ru/venano
- ID: 693866
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Resumo
The effect of temperature on the structure of single crystals of tris(ethylenediamine)nickel(II)dichloride dihydrate [Ni(en)3]Cl2·2H2O, or [Ni(H2NCH2CH2NH2)3]Cl2·2H2O, was investigated. The rearrangement of the structure with a decrease in temperature from 293 to 85 K was studied using X-ray structural analysis. A threefold decrease in the volume of the unit cell of the crystal was found while maintaining the space group C2/c.
Sobre autores
N. Sorokina
Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”
Email: nsor@crys.ras.ru
Moscow, 119333 Russia
V. Komornikov
Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”Moscow, 119333 Russia
I. Verin
Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”Moscow, 119333 Russia
N. Novikova
Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”
Email: natnov@crys.ras.ru
Moscow, 119333 Russia
Bibliografia
- Виноградов А.Н., Егоров В.В., Калинин А.П. и др. Линейка гиперспектральных сенсоров оптического диапазона. Препринт ИКИ РАН. Пр-2176. М.: ИКИ РАН, 2015. 20 с. http://www.iki.rssi.ru/books/2014egorov.pdf
- Маноменова В.Л., Руднева Е.Б., Волошин А.Э. // Успехи химии. 2016. Т. 85. № 6. С. 586. https://doi.org/10.1070/RCR4530
- Зайнуллин О.Б., Сорокина Н.И., Коморников В.А. и др. // Кристаллография. 2021. Т. 66. № 3. С. 482. https://doi.org/10.31857/S0023476121030310
- Rigaku Oxford Diffraction, CrysAlisPro Software System, Version 42.74a. 2018. Rigaku Corporation, Oxford, UK.
- Petricek V., Dusek M., Palatinus L. // Z. Kristallogr. 2014. V. 229. № 5. P. 345. https://doi.org/10.1515/zkri-2014-1737
- Palatinus L. // Acta Cryst. В. 2013. V. 69. P. 1. https://doi.org/10.1107/S2052519212051366
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