Ce0.9(Mg,Ni)0.1O2: Composite or Solid Solution

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Рұқсат ақылы немесе тек жазылушылар үшін

Аннотация

Samples of the composition Ce0.9(Mg1 – xNix)0.1O2 (0 ≤ x ≤ 1, step x = 0.1) have been obtained by gel combustion followed by hydrothermal treatment. X-ray powder diffraction data have showed that after gel combustion and annealing at 1100°C, composite CeO2 (fluorite structure)/solid solution Mg1 – xNixO (halite structure) is formed, and additional hydrothermal treatment followed by annealing promotes the formation of limited solid solution Ce0.9(Mg1 – xNix)0.1O2. According to the results of IR spectroscopy, the CeO2/Mg1 – xNixO composite does not adsorb CO2 even in the presence of water vapor, which is also confirmed by diffuse reflectance spectra in the UV-visible region. On the contrary, the Ce0.9(Mg1 – xNix)0.1O2 solid solution absorbs CO2, as evidenced by the results of IR spectroscopy and thermogravimetric analysis.

Авторлар туралы

M. Smirnova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

G. Nipan

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: gbuzanov@yandex.ru
Russian Federation, 119071, Moscow

M. Kop’eva

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

G. Nikiforova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

G. Buzanov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

E. Kozhukhova

National Research Center “Kurchatov Institute,” IREA

Email: smirnova_macha1989@mail.ru
107076, Moscow, Russia

I. Kozerozhets

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

A. Yapryntsev

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

A. Arkhipenko

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

M. Doronina

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: smirnova_macha1989@mail.ru
119991, Moscow, Russia

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© М.Н. Смирнова, Г.Д. Нипан, М.А. Копьева, Г.Е. Никифорова, Г.А. Бузанов, Е.И. Кожухова, И.В. Козерожец, А.Д. Япрынцев, А.А. Архипенко, М.С. Доронина, 2023