Copper(II) succinate: electrochemical synthesis, characterization and application as a precursor for micron-sized copper(II) oxide fibers

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A coordination compound of copper(II) with succinic acid was obtained by electrochemical synthesis in media of various compositions. The samples were characterized by methods of quantitative analysis, ESR and IR spectroscopy, synchronous thermal analysis. The vibrational frequencies of copper(II) succinate were calculated by using DFT and the experimental IR spectra were interpreted on the basis of the results. Micro-sized copper(II) oxide fibers were obtained by thermal decomposition of synthesized samples. It was shown that the use of the water–dimethyl sulfoxide system with a volume ratio 1:1 is optimal to achieve the formation of moderately aggregated particles with a distinct filamentous morphology.

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作者简介

E. Andriychenko

Kuban State University

编辑信件的主要联系方式.
Email: leka91@mail.ru
ORCID iD: 0000-0002-2324-8987
俄罗斯联邦, Krasnodar

V. Zelenov

Kuban State University

Email: leka91@mail.ru
ORCID iD: 0000-0003-3031-3844
俄罗斯联邦, Krasnodar

A. Bespalov

Kuban State University

Email: leka91@mail.ru
ORCID iD: 0000-0002-9829-9674
俄罗斯联邦, Krasnodar

V. Bovyka

Kuban State University

Email: leka91@mail.ru
ORCID iD: 0000-0001-9419-0818
俄罗斯联邦, Krasnodar

Е. Panina

Kuban State University

Email: leka91@mail.ru
俄罗斯联邦, Krasnodar

V. Volynkin

Kuban State University

Email: leka91@mail.ru
ORCID iD: 0000-0002-3352-9862
俄罗斯联邦, Krasnodar

N. Bukov

Kuban State University

Email: leka91@mail.ru
ORCID iD: 0000-0001-8559-110X
俄罗斯联邦, Krasnodar

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2. Fig.1. EPR spectrum of a polycrystalline CuSuc–3 sample at 298 K.

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3. Fig.2. Optimized structure of a fragment of the copper(II) succinate polymer chain, calculation at the B3LYP-D3BJ/6-311G(d,p) level.

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4. Fig.3. TG–DSC curves for the CuSuc–3 sample.

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5. Fig.4. Electron microscopic images of fibers of the CuSuc–1 sample (a) and copper oxide obtained by its thermolysis at 400 (b) and 500°C (c).

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6. Fig.5. Electron microscopic images and histograms of the size distribution of copper(II) oxide microfibers: CuO–1 (a), CuO–2 (b), CuO–3 (c).

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